萃取法測(cè)定地表水中揮發(fā)酚的監(jiān)測(cè)分析要點(diǎn)研究

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文章編號(hào)：1674-6139（2025）05-0135-04

中圖分類號(hào)：X832文獻(xiàn)標(biāo)志碼：B

KeyPoints for Monitoring and Analysis of Volatile Phenols in Surface Water using Extraction Method

WangJialong1，LiuRui1，MaYukun2

（1.Microbiology Research Institute，Heilongjiang Academy of Sciences，Harbin 150010，China; 2.HeilongjiangProvincial Environmental MonitoringCenter，Harbin15oo9O，China）

Abstract：ThisarticleliststhemainanalyticalmethodsnddetectionlimitsfordeterminingvolatilephenolsathomeandabroadAt present，the4aminoantipineextractionspectrophotometricmetodisteainmtodfodetermigvolatilepenolsinsufacete whichisaclasicmethod.Thismethodhashghsensitivitygodprecisionandacuracy，buttherearealsomanyinfluencingfactors. Thisarticleconductsanin-depthanalysisofthinfuencingfactorsofthedeterminationofvolatilephenolsinsurfacewaterItstudies anddiscussesfromaspectssuchasreagentsandtheirpuriy，interferenceeffects，therderofreagentadition，theinfluenceof pH on colordevelopmentesults，ndthechangesofsmplesovertime.Itprovidesotherprecautiostatecttheeterinationresultsiex periments and the purification method of 4- aminoantipyrine reagent.This ensures the smooth process of the 4-aminoantipyrine extraction spectrophotometric experiment and guarantees the accuracy of the monitoring results.

Key words：4-aminoantipyrine；volatile phenols；extraction；influencing factors；interfering substances

前言

根據(jù)酚類是否能隨水蒸氣蒸餾而出分為揮發(fā)酚和不揮發(fā)酚，沸點(diǎn)在 230% 以下隨水蒸氣蒸餾出的為揮發(fā)酚[1]。（剩余3371字）